Iron Catalysis: Fundamentals and Applications by Juan I. Padrón, Víctor S. Martín (auth.), Bernd Plietker

By Juan I. Padrón, Víctor S. Martín (auth.), Bernd Plietker (eds.)

Juan I. Padrón and Víctor S. Martín: Catalysis via Fe-based Lewis acids; Hiroshi Nakazawa*, Masumi Itazaki: Fe–H Complexes in Catalysis; Kristin Schröder, Kathrin Junge, Bianca Bitterlich, and Matthias Beller: Fe-catalyzed Oxidation Reactions of Olefins, Alkanes and Alcohols: Involvement of Oxo- and Peroxo Complexes; Chi-Ming Che, Cong-Ying Zhou, Ella Lai-Ming Wong: Catalysis by means of Fe=X Complexes (X=NR, CR2); René Peters, Daniel F. Fischer and Sascha Jautze: Ferrocene and part Sandwich Complexes as Catalysts with Iron Participation; Markus Jegelka, Bernd Plietker: Catalysis by way of advanced Ferrates.

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A plausible mechanism implies the activation of the olefin by coordination of the metal triflate followed by nucleophilic attack of the acetylene or acetylide (Scheme 31). H R C=C [Fe3+] R H + + [Fe2+] C–C [Fe2+] C–C Scheme 31 Possible mechanism of iron(III)catalyzed alkyne addition to alkenes H R Catalysis by Means of Fe-Based Lewis Acids 21 FeX3 was also found to be an excellent promoter in the classical Prins cyclization (Scheme 10, route H), with the observation of a satisfactory reaction between 3-buten-1-ol and several aldehydes, affording the corresponding cis-4-halo-2-alkyl tetrahydropyrans in good yields [Eq.

2 Photochemical Reduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72 Appendix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74 References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76 H. Nakazawa (*) and M. jp 28 H. Nakazawa and M. Itazaki 1 Introduction This chapter treats iron complexes with Fe–H bond(s).

50 4 Organic Synthesis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 C–C and C–E Bond Formation . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Others . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59 5 Hydrogen Generation . . . . . . . . . . . . . . . . . . . . . . . . .

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